Laser flash analysis
File:LFA 427.JPG | |
Uses | to measure thermal diffusivity, thermal conductivity, specific heat, |
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The laser flash analysis or laser flash method is used to measure thermal diffusivity of a multiplicity of different materials. An energy pulse heats one side of a plane-parallel sample. The temperature rise on the backside due to the energy input is time-dependent detected. The higher the thermal diffusivity of the sample, the faster the energy reaches the backside. A state-of-the-art laser flash apparatus (LFA) to measure thermal diffusivity over a broad temperature range, is shown on the right hand side.
In a one-dimensional, adiabatic case the thermal diffusivity is calculated from this temperature rise as follows:
Where
- is the thermal diffusivity
- is the thickness of the sample
- is the time to the half maximum
Measurement principle
The laser flash method was developed by Parker et al. in 1961.[1] In a vertical setup a light source (e.g. laser, flashlamp) heats the sample from the bottom side and a detector on top detects the time-dependent temperature rise. For measuring the thermal diffusivity, which is strongly temperature-dependent, at different temperatures the sample can be placed in a furnace at constant temperature.
Perfect conditions are
- homogenous material,
- a homogenous energy input on the front side
- a time-dependent short pulse - in form of a Dirac delta function
Several improvements on the models have been made. In 1963 Cowan takes radiation and convection on the surface into account.[2] Cape and Lehman consider transient heat transfer, finite pulse effects and also heat losses in the same year.[3] Blumm and Opfermann improved the Cape-Lehman-Model with high order solutions of radial transient heat transfer and facial heat loss, non-linear regression routine in case of high heat losses and an advanced, patented pulse length correction.[4][5]